Title: Standard operating procedure of Ferric
Ammonium Sulphate Solution R5.
1.0 OBJECTIVE:
To
lay down the procedure of Ferric
Ammonium Sulphate Solution R5 for Laboratory use.
2.0 SCOPE:
This
shall be applicable to the Quality Control Laboratory.
3.0 RESPONSIBILITY:
3.1
Q.C Pharmacist.
4.0 ACCOUNTABILITY:
4.1
Manager-Quality
Control.
4.2
Head of the Q.C
Department.
5.0 MATERIAL AND
EQUIPMENT:
5.1
Glassware (one 100.0ml
beaker, one stirrer, one pipette).
5.2
Analytical
weighing balance.
5.3
30.0g of Ferric Ammonium Sulphate Solution R.
5.4
40.0ml of nitric
acid R.
5.5
Purified water
(q.s).
6.0 PROCEDURE:
6.1
Weigh 30.0g of Ferric Ammonium Sulphate Solution R;
operate analytical weighing balance according to SOP.
6.2
Take a beaker of
100.0ml.
6.3
Add 30.0g of Ferric Ammonium Sulphate Solution R
with 40.0ml of nitric acid R.
6.4
Shake it by using
magnetic stirrer.
6.5
Dilute it to
100.0ml with purified water.
6.6
If the solution is
turbid, centrifuge or filter it, by using filtration apparatus.
7.0 REVISION LOG:
|
Revision No.
|
Effective Date
|
Reason
|
|
00
|
|
New
SOP
|
8.0 REFERENCES:
8.1 The British Pharmacopoeia. Vol V. Appendix I, Official Monograph /General Reagent: 2015,
pp.19-141.
9.0 ANNEXURES:
9.1
Not Applicable.
10.0
ABBREVIATIONS:
|
Abbreviation
|
Expanded Form
|
|
SOP
|
Standard operating
procedure
|
|
&
|
And
|
|
No.
|
Number
|
|
Ltd.
|
Limited
|
|
Q.C
|
Quality control
|
|
QCR
|
Quality control reagent
|
|
ml
|
Milliliter
|
|
g
|
Grams
|
|
mg
|
Milligram
|
|
R
|
Reagent
|
|
Vol
|
Volume
|
|
q.s
|
Quantity sufficient
|
No comments:
Post a Comment