Ferric Ammonium Sulphate Solution R5 Reagent Preparation SOP


Title: Standard operating procedure of Ferric Ammonium Sulphate Solution R5.
1.0  OBJECTIVE:
To lay down the procedure of Ferric Ammonium Sulphate Solution R5 for Laboratory use.
2.0  SCOPE:
This shall be applicable to the Quality Control Laboratory.
3.0  RESPONSIBILITY:
3.1  Q.C Pharmacist.
4.0  ACCOUNTABILITY:
4.1  Manager-Quality Control.
4.2  Head of the Q.C Department.
5.0  MATERIAL AND EQUIPMENT:
5.1  Glassware (one 100.0ml beaker, one stirrer, one pipette).
5.2  Analytical weighing balance.
5.3  30.0g of Ferric Ammonium Sulphate Solution R.
5.4  40.0ml of nitric acid R.
5.5  Purified water (q.s).
6.0  PROCEDURE:
6.1  Weigh 30.0g of Ferric Ammonium Sulphate Solution R; operate analytical weighing balance according to SOP.
6.2  Take a beaker of 100.0ml.
6.3  Add 30.0g of Ferric Ammonium Sulphate Solution R with 40.0ml of nitric acid R.
6.4  Shake it by using magnetic stirrer.
6.5  Dilute it to 100.0ml with purified water.
6.6  If the solution is turbid, centrifuge or filter it, by using filtration apparatus.
7.0  REVISION LOG:
Revision No.
Effective Date
Reason
00

New SOP

8.0  REFERENCES:
8.1  The British Pharmacopoeia. Vol V. Appendix I, Official Monograph /General Reagent: 2015, pp.19-141.
9.0  ANNEXURES:
9.1  Not Applicable.
10.0    ABBREVIATIONS:
Abbreviation
Expanded Form
SOP
Standard operating procedure
&
And
No.
Number  
Ltd.
Limited
Q.C
Quality control
QCR
Quality control reagent
ml
Milliliter
g
Grams
mg
Milligram
R
Reagent
Vol
Volume
q.s
Quantity sufficient


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