Ammonium molybdate solution R5 Reagent Preparation SOP


Title: Standard operating procedure of Ammonium molybdate solution R5 preparation for laboratory use.



1.0  OBJECTIVE:
To lay down the procedure of Ammonium molybdate solution R5 for Laboratory use.
2.0  SCOPE:
This shall be applicable to the Quality Control Laboratory.
3.0  RESPONSIBILITY:
3.1  Q.C Analyst.
4.0  ACCOUNTABILITY:
4.1  Manager-Quality Control.
4.2  Head of the Q.C Department.
5.0  MATERIAL AND EQUIPMENT:
5.1  Glassware (one 50.0ml beaker, one stirrer, one 10.0ml pipette).
5.2  Analytical weighing balance.
5.3  1.0g of ammonium molybdate.
5.4  40.0ml of 15% v/v solution of sulphuric acid (i.e. 15g/100ml)
6.0  PROCEDURE:
6.1  Firstly weigh 1.0g of ammonium molybdate by using analytical weighing balance operate according to SOP.
6.2  Prepare 15% v/v solution of sulphuric acid.
6.3  Take a beaker of 50.0ml and add 1.0g of ammonium molybdate in it.
6.4  Take 40.0ml of the prepare solution of 15% v/v of sulphuric acid.
6.5  Dissolve it completely by using stirrer.
6.6  Prepare the solution daily.
7.0  REVISION LOG:
Revision No.
Effective Date
Reason
00

New SOP
8.0  REFERENCES:
8.1  The European Pharmacopoeia. Vol-1. Official Monograph /Reagents: 2015, pp.425-536.
9.0  ANNEXURES:
9.1  Not Applicable.
10.0    ABBREVIATIONS:
Abbreviation
Expanded Form
SOP
Standard operating procedure
&
And
No.
Number  
Ltd.
Limited
Q.C
Quality control
ml
Milliliter
g
Grams
%
Percentage
v/v
Volume by volume
q.s
Quantity sufficient
Vol
Volume
R
Reagent

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