Title: Standard operating procedure of Ammonium
molybdate solution R5 preparation for laboratory use.
1.0 OBJECTIVE:
To
lay down the procedure of Ammonium
molybdate solution R5 for Laboratory use.
2.0 SCOPE:
This
shall be applicable to the Quality Control Laboratory.
3.0 RESPONSIBILITY:
3.1
Q.C Analyst.
4.0 ACCOUNTABILITY:
4.1
Manager-Quality
Control.
4.2
Head of the Q.C
Department.
5.0 MATERIAL AND
EQUIPMENT:
5.1
Glassware (one 50.0ml
beaker, one stirrer, one 10.0ml pipette).
5.2
Analytical
weighing balance.
5.3
1.0g of ammonium molybdate.
5.4
40.0ml of 15% v/v
solution of sulphuric acid (i.e. 15g/100ml)
6.0 PROCEDURE:
6.1
Firstly weigh 1.0g
of ammonium molybdate by using analytical weighing balance operate according to
SOP.
6.2
Prepare 15% v/v
solution of sulphuric acid.
6.3
Take a beaker of 50.0ml
and add 1.0g of ammonium molybdate in it.
6.4
Take 40.0ml of the
prepare solution of 15% v/v of sulphuric acid.
6.5
Dissolve it completely
by using stirrer.
6.6
Prepare the
solution daily.
7.0 REVISION LOG:
|
Revision No.
|
Effective Date
|
Reason
|
|
00
|
|
New
SOP
|
8.0 REFERENCES:
8.1 The European Pharmacopoeia. Vol-1. Official Monograph /Reagents: 2015,
pp.425-536.
9.0 ANNEXURES:
9.1
Not Applicable.
10.0
ABBREVIATIONS:
|
Abbreviation
|
Expanded Form
|
|
SOP
|
Standard operating
procedure
|
|
&
|
And
|
|
No.
|
Number
|
|
Ltd.
|
Limited
|
|
Q.C
|
Quality control
|
|
ml
|
Milliliter
|
|
g
|
Grams
|
|
%
|
Percentage
|
|
v/v
|
Volume by volume
|
|
q.s
|
Quantity sufficient
|
|
Vol
|
Volume
|
|
R
|
Reagent
|
No comments:
Post a Comment