Aluminium Chloride Reagent Preparation SOP


1.0  OBJECTIVE:
1.1  To lay down the procedure of Aluminium Chloride Reagent for Laboratory use.
2.0  SCOPE:
This shall be applicable to the Quality Control Laboratory.
3.0  RESPONSIBILITY:
3.1  Q.C Pharmacist.
4.0  ACCOUNTABILITY:
4.1  Manager-Quality Control.
4.2  Head of the Q.C Department.
5.0  MATERIAL AND EQUIPMENT:
5.1  Glassware (two 100.0ml beaker, one stirrer, one 10.0ml pipette).
5.2  Analytical weighing balance.
5.3  2.0g of Aluminum chloride.
5.4  100.0ml Methanol.
5.5  5.0ml of Glacial acetic acid.
5.6  5% v/v solution of glacial acetic acid in methanol. (i.e. 5ml/100ml)
6.0  PROCEDURE:
6.1  Weigh 2.0g of aluminium chloride, operate analytical weighing balance according to SOP.
6.2  Prepare 5% v/v solution of glacial acetic acid in methanol separately in another beaker of 100.0ml.
6.3  Take a beaker of 100.0ml.
6.4  Dissolve 2.0g of aluminium chloride in 100.0ml of the above prepared solution, which is explained in point 6.2.
6.5  Ready for use.
7.0  REVISION LOG:
Revision No.
Effective Date
Reason
00

New SOP

8.0  REFERENCES:
8.1  The British Pharmacopoeia. Vol V.Appendix I, Official Monograph /General Reagent: 2015, pp.19-141.
9.0  ANNEXURES:
9.1  Not Applicable.
10.0    ABBREVIATIONS:
Abbreviation
Expanded Form
SOP
Standard operating procedure
&
And
No.
Number
Ltd.
Limited
Q.C
Quality control
ml
Milliliter
g
Grams
%
Percentage
v/v
Volume by volume
Vol
Volume


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